KMID : 1035320140410010077
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Korean Society for Dental Materials 2014 Volume.41 No. 1 p.77 ~ p.83
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Precipitation hardening by simulated complete firing and holding condition in a silver-free metal-ceramic alloy of Pd-Cu-In-Ga sysem
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Jeon Byung-Wook
Kim Sung-Min Kwon Yong-Hoon Kim Hyung-Il Seol Hyo-Joung
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Abstract
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Precipitation hardening by simulated complete firing and holding condition in a silver-free metal-ceramic alloy of Pd-Cu-In-Ga system was investigated by means of hardness test, field emission scanning electron microscopic observations, X-ray diffraction analysis and energy dispersive X-ray spectrometer analysis. Most effective condition for hardening of alloy was obtained at cooling rate of stage 1 (firing chamber opens about 70 mm) and starting temperature of 600¡É. After simulated degassing treatment, the hardness value of solution treated specimen decreased by about 20 Hv, and during the simulated complete firing cycle, such a low hardness value was maintained. By holding the specimen at 600¡É and 700¡É after simulated complete firing, the hardness increased apparently. However, the decrease in hardness by overaging occurred within 30 min at the holding temperature of 700¡É. The age-hardening of a silver-free Pd-Cu-In-Ga alloy resulted from precipitation of the CuPd phase containing Ga and In from the Pd-rich matrix.
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KEYWORD
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Precipitation hardening, Holding condition, Simulated firing cycle, Silver-free Pd-Cu-In-Ga, Metal-ceramic alloy
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